The substrates were biased by dc voltage negatively with respect to ground . the films were characterized by infrared spectra and x - ray photoelectron spectroscopy ( xps ) 薄膜成分以红外吸收谱和x射线光电子能谱标识，薄膜形貌以原子力显微镜观测。
The xps measurements confirmed the presentation of poms and doda ( ddda ) in the multibilayers . the photoluminescent spectrum exhibit characteristic photo luminescence of the eu3 + ion , basically similar to those found for the polyoxometalate solids X射线光电子能谱结果表明pom在膜中的存在，并且表明前驱体膜中的氯离子已经完全被多阴离子交换掉，这与前面的结论相一致。
The results of attenuated total reflectance - fourier transform infrared ( atr - ftir ) , x - ray photoelectron spectroscopy ( xps ) and contact angle measurement showed that the amphiphilic copolymer could self - segregate on the hydrophobic pdl - la surface 利用衰减全反射傅立叶转换红外光谱( atr - ftir ) 、 x -射线光电子能谱( xps )分析以及接触角测定对改性聚乳酸材料表面进行了表征。
The surface restoration layer of a gear wheel , which had run in lubricating oil with pbc restoration agent was analyzed using tem , sem , xps , aes and raman ; and the mechanism of reducing friction of the restoration agent was studied 以透射电镜、 x射线光电子能谱仪、俄歇电子能谱仪和拉曼光谱仪分析了在添加摩圣修复剂的润滑油中运行过的齿轮表层，对摩圣修复剂的减摩机理进行了分析。
X - ray powder diffractometer ( xrd ) , forier transform infrared spectroscopy ( ft - ir ) and crystalline parameters were used to determine the structure of the samples , x - ray photoelectron spectra ( xps ) were employed to determine the oxide state of elements in the samples X射线粉末衍射仪( xrd )和傅立叶变换红外光谱仪( ft - ir )确定了不同掺杂比样品的结构， x射线光电子能谱( xps )确定样品的价态。
By means of esca , igc , wd , dsc ) sem and computer aided image processing technique , the relations of composite ' s microsimcture and macroscopic properties were researched and conclusions were listed as follows . l 借助x射线光电子能谱( esca ) 、反相气相色谱( igc ) 、 x射线衍射分析、 dsc分析和扫描电镜( sem )等测试手段和计算机图像处理技术，分析了材料微观结构与宏观性能间的关系，取得了如下结果。
2 studying of the properties of cbn thin films afm showed that cbn thin film delaminated from substrate obviously . basing xps , we calculate the nib ratio to be 0 . 90 that is closing to unity , and the thickness of hbn layer on cbn layer that is about 0 . 80 nm 根据x射线光电子能谱，计算得到立方氮化硼薄膜中的n和b的原子数比为0 . 90 ，接近理想化学配比1 ；立方氮化硼薄膜顶层的六角氮化硼的厚度约为0 . 80nm 。
Cu ( vol20 % ) mgf2 cermet film was also sputtered and meas ured and analyzed by xps , the results showed that the volume fraction of cu was 22 . 6 % , which was very close to that of theoretical calculation and the longitudinal distribution of cu component was even 用x射线光电子能谱xps对其中某一组分cu ( vol20 ) mgf _ 2样品进行刻蚀测量表明： cu的体积百分比约为22 . 6 ，与实验预测相当接近，且样品的组分纵向分布均匀。
The formation of self - assembled interfacial n - dodecanethiol monolayer and its effect on the corrosion protection of epoxy coating were evaluated using the x - ray photoelectronic spectroscopy , electrochemical impedance spectroscopy , impedance - time transition , and phase angle - time transition method 采用x射线光电子能谱、电化学阻抗谱、阻抗时间谱和相位角时间谱等方法对硫醇自组装界面层及其对涂层腐蚀防护性能的影响进行了研究。
Two kinds of antibacterial glass material system are studied with xps , sem , spectrophotometer and atom absorb photometer , antibacterial property test and toxicity to investigate the influential factors to the antibacterial glass material and their relations 对于两种系列的抗菌玻璃材料运用x射线光电子能谱( xps ) 、扫描电镜( sem ) 、分光光度计、原子吸收光度计、抗菌测试等方法，详细的研究了影响抗菌玻璃材料的各个因素，及其相互之间的关系。
